Axis 5600plus Podręcznik Użytkownika Pobierz pdf (Strona 31)

Hardware Profiles and Projects

System User Guide

D5033331 A

AB SCIEX TripleTOF

5600/5600+ Instruments

31 of 116

4. Click Add Device.

In the Available Devices dialog, in the Device Type field, Mass Spectrometer is the

preset value (Figure 2-3).

Figure 2-3 Available Devices dialog

5. In the Devices list, select the Mass Spectrometer TripleTOF 5600 instrument and

then click OK.

6. In the Devices in current profile list, select the instrument.

7. Click Setup Device.

8. (Optional) On the Configuration tab (Figure 2-4), in the Settings for Integrated

Devices section, select the Use calibrant delivery system (CDS) check box.

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AB SCIEX TripleTOF 1
5600/5600+ 1
Instruments 1
Contents 3
General Safety Information 7
Symbols and Conventions 7
Qualified Personnel 8
Regulatory Compliance 10
International 11
IN DIAGNOSTIC PROCEDURES 12
Mains Supply 14
Laboratory Ventilation 15
Environmental Conditions 15
Electronic Equipment) 16
System Information 17
Theory of Operation 17
Data Handling 17
System Overview 18
Start Up the System 20
Shut Down the System 21
Instrument Safe Fluids 26
Sample Workflows 27
Hardware Profiles 29
Create a New Subproject 36
Copy a Subproject 36
Installed Project Folders 37
Optimize the Instrument 39
Basic Acquisition Methods 41
Add an Experiment 43
Add a Period 43
Scan Techniques 44
Single Mass Spectrometry 44
Tandem Mass Spectrometry 44
About Instrument Parameters 45
Create and Submit a Batch 51
Set up Sample Calibration 54
Acquire Data 55
(Optional) 57
Stop Sample Acquisition 57
Batch Editor Right-Click Menu 58
Queue States 59
Queue Right-Click Menu 62
Analyzing and Processing Data 65
Show Experimental Conditions 66
Show ADC Data 67
Chromatograms 68
Show TICs from a Spectrum 69
Show a Spectrum from a TIC 69
Generate XICs 69
Generate BPCs 72
Generate XWCs 74
View DAD Data 74
Generate TWCs 74
Adjust the Threshold 75
Data Processing 77
Zoom in on the y-axis 79
Zoom in on the x-axis 79
TurboIonSpray Probe 84
APCI Probe 85
Ion Source Latch 86
Source Exhaust System 86
Installation 87
Install the Ion Source 88
Optimization 89
Run the Method 90
Set the Starting Conditions 90
Optimize the APCI Probe 92
Maintenance 95
Remove the Ion Source 96
Remove the Probe 96
Clean the Electrode Tube 97
Replace the Electrode 98
0.5 - 1 mm 99
Replace the Sample Tubing 100
Troubleshooting 101
Consumables 102
Cleaning and Maintenance 103
Health and Safety Precautions 103
Clean the Surfaces 104
Empty the Drain Bottle 104
Front-End Cleaning 105
Best Practices 106
Prepare for Routine Cleaning 107
Clean the Curtain Plate 108
Basic System Troubleshooting 111
Recommended Calibration Ions 113

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