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Rows after the first row of the spreadsheet contain the programmed settings for
each of the ramp segments. Each segment will ramp to the specified pressure at
the specified rate (assuming the rate is achievable), and then hold the pressure
for the specified time. (Note that the Rate in the first row is always blank and
cannot be edited. Also note that the entire Total column cannot be edited.)
Constant Column Flow for Type 1 EFC
Constant Column Flow mode for Type 1 EFC is enabled in the Flow/Pressure
section.
Click on the Radio Button to turn on the Constant Column Flow Mode. This mode
disables the spreadsheet and reveals the constant flow rate value.
Enter the desired Column Flow.
Click on “Yes” to perform a pressure pulse injection. Upon injection, the pressure will
change to the Pulse Pressure for the Pulse Duration setting.
When the method is activated in System Control, the Varian MS Workstation will
generate and download the appropriate pressure program corresponding to the
Column Temperature program, the Column Setup Length and Diameter, the
Carrier Gas, and the ambient Barometric Pressure. These parameters are
specified in the 3900 GC system control setup, and the Barometric Pressure is
measured by the 3900 at the time the Method is downloaded. The 3900 will run
the pressure program to hold the Column Flow at the specified value as the
Column Temperature is ramped during each run.
Injector Section
Use the Injector Program to specify the temperature setpoints of the isothermal
1177 Injector, and split ratio of the 1177 Injector.
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